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PDF (601 kb) 2 Sample Preparation and Measurement of Spectra ... 5 Combination of 1 H and 13 C NMR Spectroscopy Full Text; PDF (23279 kb) 6 NMR of other Nuclei Full ... General methods: 1H NMR spectra were measured on a Varian Mercury-300 (300 MHz) spectrometer at ambient temperature. ... HRMS(FAB+) calcd for C40H26O4P [M+H]+ 601 ...